화학공학소재연구정보센터
Molecular Crystals and Liquid Crystals, Vol.588, No.1, 83-94, 2014
Synthesis, Crystal Structure, and Characterization of New 2,4,5-Triphenyl Imidazole: 4,5-Diphenyl-2-(3,4,5-trimethoxyphenyl)-1H-imidazole
The substituted triarylimidazole, C24H22N2O3, was prepared from the three-component one-pot condensation reaction and the product was crystallized by using dimethylformamide. The structure of the compound was confirmed by elemental analysis, FT-IR, thermogravimetric analysis (TGA), UV-Visible and single-crystal X-ray diffraction. The compound crystallizes in the monoclinic crystal system in the space group P2(1)/c with unit cell parameters a = 10.509(3) angstrom, b = 18.748(5) angstrom, c = 22.016(6) angstrom, = 90.844(5)degrees, and Z = 8. The crystal structure of the compound was stabilized by the inter-molecular interactions of types N-HN, C-HO, and C-HN, and intra-molecular interactions of the type C-HO. The structure also involves C-H interactions.